|
Eden Labs LLC supports a variety of different
methods for performing extracts. Please review these methods
to decide which systems applies to your needs. Feel free to
call or E-mail any questions you may have.
THE COLDFINGER METHOD
DISTILLATION/EXTRACTION
This is the original extraction method that Eden Labs was
built on and it continues to be the backbone of the company.
Technically, our distillation devices are "modified soxhlet
extracters." The original soxhlet extracter was developed by
Franz Von Soxhlet, a German agricultural chemist, in the
early part of this century. Our patent pending modifications
to his basic design make it possible for the operater to
distill at much lower temperatures and it enables one to
recollect the solvent that was used to extract the plant
material back out of the extract for re-use.
Within an enclosed flask there is an inverted
condenser pointing down into the flask from the top. Just
below that condenser will be suspended either what's called
a soxhlet basket or a recovery vessel depending on whether
you're extracting or recovering solvent. The condenser will
have cold liquid circulating through it to keep the
condenser cold. In the bottom of the main flask solvent is
placed. To do an extraction, the ground plant material is
placed in the soxhlet basket which is a vessel with
perforated sides and bottom so that liquid can fall through
it. When gentle heat is applied to the main flask, the
solvent begins to evaporate and the solvent vapors reach the
cold condenser at the top of the flask and begin to liquefy
on the sides of the condenser. (much the same way that a
cold glass of water becomes wet on the outside of itself on
a hot day) The re-condensed solvent on the sides of the
condenser begin flowing down the sides of the condenser and
begin dripping off of drip points on the end of the
condenser. This solvent drips into the top of the soxhlet
basket where it saturates the herb being extracted. The
solvent flows through the basket and out the holes in the
bottom of the basket carrying the extract with it into the
bottom of the flask.
The extract laden solvent falling from the soxhlet basket
is dark in color and as it becomes clearer you know that the
plant material is leached out and the process is
finished.
At this point you can do one of three things: 1.
Stop the operation and pour the extract infused solvent out
of the main flask. 2. Hook up the recovery vessel and remove
the solvent from your extract which generally leaves a paste
behind. 3. Dump and squeeze out the spent plant material in
the soxhlet basket, then start a fresh basket of herb in the
extracter using the same solvent which continually
re-distills and extracts regardless of how much extract is
infused into it in the bottom of the main flask.
The recovery vessel is simply a cup which is
suspended below the condenser. As solvent vapors re-condense
and fall off the tip of the condenser, they fall into the
cup and are thus separated from the extract itself.
Our most sophisticated units which use this process
are also vacuum compatible. Applying a vacuum to this inside
of the main flask lowers the boiling point of the solvent
enabling the operator to distill solvent at much lower
temperatures and to distill much more quickly. When using
vacuum, solvent vapors will migrate out of the port through
which the vacuum is being pulled. To capture these vapors
before they go into the vacuum pump, a cold trap is utilized
which is a different type of condenser which re-condenses
solvent vapors and then sends the liquid solvent back into
the main flask. (see Professional Round Bottom unit)
COLD PERCOLATION
This is a traditional method of extraction used by
herbalists throughout the world and it's very simple. Above
a flask or vessel is suspended a cone or tube. The bottom of
the tube has a perforated base which holds ground herb in
place. Solvent is poured into the top of the tube where it
soaks through the herb leaching out the extract and then
falling out the bottom end of the tube into the flask. If
desired, the percolation tube can be wrapped in heating tape
to help facilitate the extraction.
Percolater cones or tubes can be ordered as
accessories to any of our basic distillation units. Please
contact us for details and prices as these our custom made
to customer request.
AGITATION/DISTILLATION
This is the accepted method used by most large,
industrial operations which are in the business of
processing herbal extracts. The main reason for this is that
the distillation/extraction method outlined earlier becomes
cost prohibitive and very time consuming when sized up to
industrial scale.(Our largest distillation/extraction unit
is the size of a 55 gallon drum. Beyond this size, that
design becomes impractical.)
The first stage of this process involves the use of
a large mixing vat or tank. The tank is heated by a water
jacket and has a big mixing arm with blades on it extending
down through the top of it. Ground herb and solvent are put
in the tank and agitated for a determined period of time. In
the bottom of the tank is a three-way valve. During
agitation the valve is closed. After agitation, the valve is
opened to let the liquid out but the plant material is
retained for further agitation. The liquid that is recovered
from this first run is very thick with extract and is
suitable for immediate use if a liquid extract is the
desired form.
To completely leach out the plant material, more
solvent must be introduced into the agitation vessel whereby
the process is repeated. This process may be repeated 2-4
times to completely leach out the extract from your herb
with each successive run yielding a leaner batch of extract.
When the last run is complete, the valve is opened up so
that the spent herb and the solvent all run out thus
draining the tank. To recover the solvent from these batches
of extract, a distillation vessel is used to strip the
solvent out of the extract similar to the solvent recovery
method outlined in the distillation/extraction section. A
press or centrifuge is used to squeeze the liquid out of the
spent plant material.
High Pressure- Supercritical/Subcritical
Extraction
This is the most technologically advanced extraction
system in the world. Research into the techniques and
applications of this amazing process is ongoing and Eden
Labs is at the forefront of these investigations.
Super Critical Fluid Extraction (SFE) involves
taking gases, usually CO2, and compressing them into a dense
liquid. This liquid is then pumped through a cylinder
containing the material to be extracted. From there, the
extract laden liquid is pumped into a separation chamber
where the extract is separated from the gas and the gas is
recovered for re-use. CO2 's solvent properties can be
manipulated and adjusted by varying the pressure and
temperature that one works at.
The advantages of SFE are the versatility it offers
in pinpointing the constituents you want to extract from a
given material and the fact that your end product has
virtually no solvent residues left in it. (CO2 evaporates
completely) The downside is that this technology is quite
expensive.
There are many other gases and liquids that are highly
efficient as extraction solvents when put under pressure.
Please click on our section titled High Pressure
Supercritical Fluid Extraction for more details.
herbs, ethanol, fuel ethanol, herbal extraction,
extractor, herbal, herbal extractor, distillation,
distillation equipment, solvent recovery, solvent, chemical
recovery, supercritical fluid extractor, alkaloid, alkaloid
extraction, essential oil, coldfinger, Eden Labs,
extraction, health food, laboratory supplies, glassware,
chemistry, vacuum, vacuum pumps, supercritical fluid
extraction
|